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12
Anions
14
Cations
31
Salts

Revision Guide

Quick recap for Anion & Cation Analysis

A

Dilute H₂SO₄ Group

Reagent: Dilute Sulphuric Acid

CO₃²⁻Carbonate

A colourless, odourless gas is evolved with brisk effervescence, which turns lime water milky.

Gas: CO₂
S²⁻Sulphide

Colourless gas with the smell of rotten eggs is evolved which turns lead acetate paper black.

Gas: H₂S
SO₃²⁻Sulphite

Colourless gas with a pungent smell, like burning sulphur which turns acidified potassium dichromate solution green.

Gas: SO₂
NO₂⁻Nitrite

Brown fumes which turn acidified potassium iodide solution containing starch solution blue.

Gas: NO₂
CH₃COO⁻Acetate

Colourless vapours with smell of vinegar. Vapours turn blue litmus red.

Gas: CH₃COOH vapours
B

Concentrated H₂SO₄ Group

Reagent: Conc. Sulphuric Acid

Cl⁻Chloride

A colourless gas with pungent smell, which gives dense white fumes when a rod dipped in ammonium hydroxide is brought near the mouth of the test tube.

Gas: HCl
Br⁻Bromide

Reddish brown gas with a pungent odour is evolved. Intensity of reddish gas increases on heating the reaction mixture after addition of solid MnO₂ to the reaction mixture. Solution also acquires red colour.

Gas: Br₂ vapours
I⁻Iodide

Violet vapours, which turn starch paper blue and a layer of violet sublimate is formed on the sides of the tube. Fumes become dense on adding MnO₂ to the reaction mixture.

Gas: I₂ vapours
NO₃⁻Nitrate

Brown fumes evolve which become dense upon heating the reaction mixture after addition of copper turnings and the solution acquires blue colour.

Gas: NO₂
C₂O₄²⁻Oxalate

Colourless, odourless gas is evolved which turns lime water milky and the gas coming out of lime water burns with a blue flame, if ignited.

Gas: CO and CO₂
I

Independent Group

No specific group reagent

SO₄²⁻Sulphate

Tested directly using specific confirmatory tests (BaCl₂ for Sulphate, Ammonium Molybdate for Phosphate).

PO₄³⁻Phosphate

Tested directly using specific confirmatory tests (BaCl₂ for Sulphate, Ammonium Molybdate for Phosphate).