JEE Main · 2024 · Shift-IImediumPOC-006

Chromatographic technique/s based on the principle of differential adsorption is/are A. Column chromatography B. Thin…

Practical Organic Chemistry · Class 11 · JEE Main Previous Year Question

Question

Chromatographic technique/s based on the principle of differential adsorption is/are A. Column chromatography B. Thin layer chromatography C. Paper chromatography Choose the most appropriate answer from the options given below:

Options
  1. a

    B only

  2. b

    A only

  3. c

    A & B only

  4. d

    C only

Correct Answerc

A & B only

Detailed Solution

Step 1: Define Differential Adsorption

Differential adsorption means different compounds adsorb on a solid adsorbent surface with different strengths. More polar compounds interact more strongly with a polar adsorbent (like silica gel or alumina), while less polar compounds adsorb weakly.

Step 2: Analyse Each Technique

A. Column Chromatography

  • Stationary phase: solid adsorbent (silica gel or alumina) packed in a glass column
  • Mobile phase: liquid solvent (eluent)
  • Separation mechanism: differential adsorption — components travel at different speeds through the column
  • Less polar compounds elute first; more polar ones are retained longer

B. Thin Layer Chromatography (TLC)

  • Stationary phase: thin layer of silica gel or alumina coated on a glass/aluminium plate
  • Mobile phase: liquid solvent
  • Separation mechanism: same differential adsorption principle as column chromatography
  • Used for quick qualitative analysis and monitoring reactions

C. Paper Chromatography

  • Stationary phase: water absorbed in cellulose fibres of the paper (a liquid stationary phase)
  • Separation mechanism: differential partition between mobile organic solvent and stationary water film
  • This is partition chromatography, NOT adsorption chromatography

Step 3: Summary Table

| Technique | Stationary Phase | Principle | |---|---|---| | Column chromatography | Solid (silica gel / alumina) | Differential adsorption ✅ | | TLC | Solid (silica gel / alumina) | Differential adsorption ✅ | | Paper chromatography | Liquid (water in cellulose) | Differential partition ❌ |

Step 4: Conclusion

Only A and B are based on differential adsorption → Option (c) A & B only

Key Points to Remember:

  • Column chromatography and TLC: adsorption principle (solid adsorbent)
  • Paper chromatography: partition principle (liquid stationary phase)
  • Polar compound → stronger adsorption → lower RfR_f → elutes last
  • Silica gel and alumina are the two standard polar adsorbents in organic chemistry

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